𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Degree of conversion and mechanical properties of a BisGMA:TEGDMA composite as a function of the applied radiant exposure

✍ Scribed by Fernanda C. Calheiros; Márcia Daronch; Frederick A. Rueggeberg; Roberto R. Braga


Publisher
John Wiley and Sons
Year
2008
Tongue
English
Weight
135 KB
Volume
84B
Category
Article
ISSN
1552-4973

No coin nor oath required. For personal study only.

✦ Synopsis


Abstract

Objective: Verify the influence of radiant exposure (H) on composite degree of conversion (DC) and mechanical properties. Methods: Composite was photoactivated with 3, 6, 12, 24, or 48 J/cm^2^. Properties were measured after 48‐h dry storage at room temperature. DC was determined on the flat surfaces of 6 mm × 2 mm disk‐shaped specimens using FTIR. Flexural strength (FS) and modulus (FM) were accessed by three‐point bending. Knoop microhardness number (KHN) was measured on fragments of FS specimens. Data were analyzed by one‐way ANOVA/Tukey test, Student's t‐test, and regression analysis. Results: DC/top between 6 and 12 J/cm^2^ and between 24 and 48 J/cm^2^ were not statistically different. No differences between DC/top and bottom were detected. DC/bottom, FM, and KHN/top showed significant differences among all H levels. FS did not vary between 12 and 24 J/cm^2^ and between 24 and 48 J/cm^2^. KHN/bottom at 3 and 6 J/cm^2^ was similar. KHN between top and bottom was different up to 12 J/cm^2^. Regression analyses having H as independent variable showed a plateau region above 24 J/cm^2^. KHN increased exponentially (top) or linearly (bottom) with DC. FS and FM increased almost linearly with DC/bottom up to 55% conversion. Conclusions: DC and mechanical properties increased with radiant exposure. Variables leveled off at high H levels. © 2007 Wiley Periodicals, Inc. J Biomed Mater Res Part B: Appl Biomater, 2008


📜 SIMILAR VOLUMES


Effect of photoactivation protocol and r
✍ F. Gonçalves; F. C. Calheiros; M. F. Witzel; Y. Kawano; R. R. Braga 📂 Article 📅 2007 🏛 John Wiley and Sons 🌐 English ⚖ 91 KB

## Abstract The use of soft‐start photoactivation to reduce shrinkage stress has become widespread in restorative dentistry. However, an increased susceptibility to ethanol degradation of polymers formed by pulse‐delay photoactivation was reported. It was hypothesized that reductions in flexural st

Copolymer composition as a function of m
✍ Francis M. Mirabella Jr.; Edward M. Barrall II; Edmund F. Jordan Jr.; Julian F. 📂 Article 📅 1976 🏛 John Wiley and Sons 🌐 English ⚖ 340 KB 👁 3 views

## Abstract The copolymer compositions as a function of molecular weight for three poly(styrene‐co‐vinyl stearate) copolymers of widely varying conversion were determined. A combined gel permeation chromatography–infrared spectroscopy method was used. Theoretical changes in copolymer composition we

Linearized frequency conversion properti
✍ A. Cidronali; G. Loglio; G. Manes 📂 Article 📅 2006 🏛 John Wiley and Sons 🌐 English ⚖ 463 KB

In this article a technique that allows derivation of the conversion matrix of a two-port device using a measurement setup based on a nonlinear vector network analyzer (NVNA), which is capable of identifying the optimum local oscillator (LO) level and the corresponding RF and IF terminations for a m

Nanomechanical properties of self-reinfo
✍ Debra D. Wright-Charlesworth; William J. Peers; Ibrahim Miskioglu; Laura L. Loo 📂 Article 📅 2005 🏛 John Wiley and Sons 🌐 English ⚖ 142 KB

## Abstract Understanding the wear characteristics of bone cement and its alternatives is critical to improving the quality and longevity of hip replacements. A novel composite material, self‐reinforced composite poly(methyl methacrylate), has been previously developed for potential use as a pre‐co

The micro-Raman spectroscopy, a useful t
✍ Pianelli, C. ;Devaux, J. ;Bebelman, S. ;Leloup, G. 📂 Article 📅 1999 🏛 John Wiley and Sons 🌐 English ⚖ 94 KB 👁 2 views

Light-activated composites are now among the most popular dental restorative materials. Nevertheless, concerns exist about the so-called depth of cure. Infrared spectroscopy (FTIR) has traditionally been used to quantify this problem by evaluating the degree of conversion of dental resins. However,