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Cyanoacetylation of 6-aminouracils. Synthesis of 7-aminopyrido[2,3-d]pyrimidine-2,4,5-triones

✍ Scribed by N. M. Smirnova; N. M. Cherdantseva; O. A. Burova; V. M. Nesterov; T. S. Safonova


Publisher
Springer US
Year
1990
Tongue
English
Weight
337 KB
Volume
26
Category
Article
ISSN
0009-3122

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Oxo-l,2,4.triazoio[4,3-a]quinoline.9-carboxylic Acid Anilide (Vllb). A mixture of 2.78 g (10 mmole) of anilide IIc, 0.72 g (12 mmole) of urea, and 30 ml of ethylene glycol was refluxed, after which it was cooled, and the resulting precipitate was reerystaUized.