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Cuprous chloride-modified columns for gas-liquid chromatography of olefins [1]

✍ Scribed by Subbarao, K. V. ;Damodaran, N. P. ;Dev, Sukh

Book ID
102346155
Publisher
John Wiley and Sons
Year
1981
Tongue
English
Weight
158 KB
Volume
4
Category
Article
ISSN
0935-6304

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✦ Synopsis

Gas chromatography 10O/0 CuCl in stationary phase greatly improves resolution of high-boiling olefins (up to 190OC)

a) For other GLC parameters see foot note, Table 1 b, Ref. 191

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The extract was filtered and the filtrate diluted with an equal volume of water. 50 ml strong solution of lead subacetate was added and the mixture centrifuged after 5 minutes. Excess lead was precipitated with 10% disodium hydrogen phosphate and the mixture again centrifuged. The supernatant was su