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Cu-silicalite-1 catalyst for the wet hydrogen peroxide oxidation of phenol

✍ Scribed by T. Granato; A. Katovic; K. Maduna Valkaj; A. Tagarelli; G. Giordano

Publisher
Springer
Year
2008
Tongue
English
Weight
410 KB
Volume
16
Category
Article
ISSN
1380-2224

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## Abstract The hydroxylation of benzene to phenol with hydrogen peroxide was investigated using different solvents and a series of catalysts, obtained by modification of titanium silicalite (TS‐1). The best results were obtained after post‐synthesis treatment of TS‐1 with NH~4~HF~2~ and H~2~O~2~.

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The promoted wet air oxidation of phenol has been investigated through the addition of hydrogen peroxide as a source of free radicals. The reaction has been shown to proceed in two stages, an initial fast reaction associated with hydrogen peroxide consumption and a second slower step that occurs at