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Crystallographic Studies of Dehydration Phenomenon in Methyl 3-hydroxy-2-methyl-1,1,4-trioxo-1,2,3,4-tetrahydro-1λ6-benzo[e][1,2]thiazine-3-carboxylate

✍ Scribed by Muhammad Nadeem Arshad,Onur Şahin…


Book ID
126358558
Publisher
Springer
Year
2013
Tongue
English
Weight
384 KB
Volume
43
Category
Article
ISSN
1572-8854

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Methyl 4-(4-hydroxy-3-methoxyphenyl)-6-m
✍ Shang, Zhen-Hua ;Ha, Jing 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 865 KB

The title compound, C 14 H 16 N 2 O 4 S, was synthesized by the reaction of 4-hydroxy-3-methoxybenzaldehyde, thiourea and methyl 3-oxobutanoate in ethanol under reflux. The crystal structure is stabilized mainly through intermolecular N-HÁ Á ÁS and O-HÁ Á ÁO hydrogen bonds. The tetrahydropyrimidin-2