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Crystal Structure Refinement of Lead Cyanamide and the Stiffness of the Cyanamide Anion

✍ Scribed by Xiaohui Liu; Andrea Decker; Dieter Schmitz; Richard Dronskowski

Publisher
John Wiley and Sons
Year
2000
Tongue
German
Weight
78 KB
Volume
626
Category
Article
ISSN
0372-7874

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✦ Synopsis

The crystal structure of lead cyanamide, PbNCN, has been refined on the basis of a single crystal grown from solution. PbNCN crystallizes in space group Pnma (Z = 4) with a = 555.66(4) pm, b = 386.77(2) pm, and c = 1173.50(8) pm. The cyanamide anion exhibits CΒ±N bond lengths of 116 pm and 130 pm, and the NΒ±CΒ±N angle is 176Β°. Quantum-chemi-cal DFT calculations indicate that the cyanamide unit is comparatively easy to distort.

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