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Crystal structure of the 1:3 thiourea-hexachloroethane inclusion compound at 295 K

✍ Scribed by S. F. Solodovnikov; G. N. Chekhova; G. V. Romanenko; N. V. Podberezskaya; Z. A. Solodovnikova; D. V. Pinakov; A. R. Semenov


Book ID
106427375
Publisher
SP MAIK Nauka/Interperiodica
Year
2007
Tongue
English
Weight
257 KB
Volume
48
Category
Article
ISSN
0022-4766

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The molecular structure of [ l.l.l]propellane has been determined from single-crystal X-ray diffraction measurements at 138 K. The crystals of this reactive compound were grown from the melt at ca. 263 K. The space group is C2, and the asymmetric unit contains four molecules. All have large thermal