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Crystal Structure of B-Type Tm2Si2O7 ( Tm4[Si3O10][SiO4]).

✍ Scribed by Ingo Hartenbach; Falk Lissner; Thomas Schleid


Publisher
John Wiley and Sons
Year
2003
Weight
73 KB
Volume
34
Category
Article
ISSN
0931-7597

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✍ M. Driess; C. von HΓ€nisch; K. Merz πŸ“‚ Article πŸ“… 1999 πŸ› John Wiley and Sons 🌐 German βš– 99 KB πŸ‘ 2 views

The compounds [(Me 3 SiO) 8 Te 2 O 2 ] (1) and [(Me 4 Si 2 O 2 ) 3 Te] (2) have been prepared in good yields through Bronsted acid-base reaction of Te(OH) 6 with Me 3 SiNEt 2 and Me 4 Si 2 (NEt 2 ) 2 , respectively. They have been characterised by multinuclear NMR spectroscopy and single crystal X-r