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Crystal Structure of 4-Trimethyltin-quinuclidinium Perchlorate

✍ Scribed by Margareta Zehnder

Publisher
John Wiley and Sons
Year
1980
Tongue
German
Weight
237 KB
Volume
63
Category
Article
ISSN
0018-019X

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✦ Synopsis

Abstract

The crystal structure of 4‐trimethyltin‐quinuclidinium perchlorate has been determined by direct methods and refined by least squares techniques. Crystals of C~10~H~22~ClNO~4~Sn are monoclinic, space group I2/c with lattice parameters a = 29.445 (13), b = 18.400(8), c = 11.300(5) Γ…, Ξ² = 95.82(5)Β°, V = 6090.65Γ…^3^, and two independent molecules (Z = 16), Interatomic distances are compared with those of known structures of quinuclidinium chloride and 4‐haloquinuclidinium chlorides and perchlorates.

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