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Crystal Structure of 2-Hydroxy-4,9-methano[11]annulenone

✍ Scribed by D. W. J. Cruickshank; G. Filippini; O. S. Mills

Publisher: John Wiley and Sons
Year: 1973
Tongue: English
Weight: 227 KB
Volume: 12
Category: Article
ISSN: 0044-8249
DOI: 10.1002/anie.197308551

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The reaction between PCl 3 and ReCl 5 yielded at 200 °C the ionic tetrachlorophosphonium dirhenium nonachloride, (PCl 4 )[Re 2 Cl 9 ]. Single crystal X-ray diffraction analysis revealed a monoclinic unit cell: a = 8.616(3) A Ê , b = 10.449(4) A Ê , c = 9.397(3) A Ê , b = 99.72(3)°, V = 833.9(5) A Ê