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Crystal structure of 1-(2,3:5,6-Di-O-isopropylidene-β-D-mannofuranosyl)-1H-[1,2,3]triazol-4,5-dicarboxylic acid diethyl ester

✍ Scribed by Harry Seibel; Penny L. Miner; Peter Norris; Timothy R. Wagner

Book ID
106403972
Publisher
Springer
Year
2007
Tongue
English
Weight
399 KB
Volume
37
Category
Article
ISSN
1572-8854

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X-ray and conformational investigation of 6-deoxy-6-C-(1,5-di-O-acetyl-2,3-O-isopropylidene-β-d-allo-pentofuranos-5-yl)-1,2:3,4-di-O-isopropylidene- α-d-galactopyranose and 6-C-(benzyl 5-deoxy-2,3-O-isopropylidene-β-d-ribofuranosid-5-yl)-1,2:3,4-di-O-isopropylidene- d-glycero-α-d-galacto-hexopyranose
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The structures of the title compounds (2b and 3) have been investigated in the solid state by X-ray methods. The crystals of 2b are monoclinic, space group P2,, and of 3 orthorhombit, space grtup P2,2,2,. The cell dimensions are: for 2b, a = 9.910(2), b = 11;745W, c = 11.810(3) A, /3 = 97.32(l)"; a

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The x-ray crystal structure of 2,3:4,5-di-O-isopropylidene-1-O-methyl-β-d-fructopyranose
✍ S.F. Watkins; S.J. Kim; F.R. Fronczek; R.J. Voll; E.S. Younathan 📂 Article 📅 1990 🏛 Elsevier Science 🌐 English ⚖ 438 KB

The molecule is a derivative of the naturally occurring carbohydrate D-fNCtOSe. The data reported here indicate that the ketose six-membered ring is constrained by the presence of two fused five-membered rings into the 3So conformation. These findings agree with the n.m.r.-spectroscopic results for