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Crystal structure determinations

✍ Scribed by Mason, S.F.

Book ID
109716736
Publisher
Nature Publishing Group
Year
1979
Tongue
English
Weight
139 KB
Volume
282
Category
Article
ISSN
0028-0836

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The trifluorophosphoranes TrtRPF 3 (R = tert.-Bu (1), Ph (2), NEt 2 (3)) were obtained by the oxidative addition of TrtF (Trt = triphenylmethyl) to the difluorophosphines RPF 2 . At room temperature only 1 exhibited dynamic behaviour in solution, but at Β±5 Β°C the pseudorotation was slow enough to pe