Crystal structure and thermal chemical properties of 2-(2,4-dimethylanilino)-3-methyl-6-diethylaminofluorane

✍ Scribed by X. M. Li; C. F. Ding; B. Q. Tian; Q. Liu; S. S. Zhang; H. Xu; P. K. Ouyang

• Book ID: 111490965
• Publisher: Versita
• Year: 2006
• Tongue: English
• Weight: 212 KB
• Volume: 60
• Category: Article
• ISSN: 0366-6352
• DOI: 10.2478/s11696-006-0039-3

✦ Synopsis

Abstract

The crystal structure of 2-(2,4-dimethylanilino)-3-methyl-6-diethylaminofluorane has been determined by single crystal X-ray diffraction method. The crystal belongs to triclinic system, space group P-1 with unit cell constants a = 11.2877(9) Å, b = 11.9539(9) Å, c = 12.2365(9) Å, α = 97.2580(10)°, β = 116.2850(10)°, γ = 106.3710(10)°, V = 1358.48(18) Å 3, Z = 2, D c = 1.234 g/cm3, μ = 0.079 mm−1, F(000) = 536, R and w(R) are 0.0718 and 0.2055, respectively, for 5239 unique reflections with 3745 observed reflections (I > 2σ(I)).