Crystal structure and solid-state behavior of aspirin anhydride crystals
β Scribed by Stephen R. Byrn; P. Y. Siew
- Publisher
- John Wiley and Sons
- Year
- 1981
- Tongue
- English
- Weight
- 394 KB
- Volume
- 70
- Category
- Article
- ISSN
- 0022-3549
No coin nor oath required. For personal study only.
β¦ Synopsis
The crystal structure and solid-state behavior of aspirin anhydride were determined using single-crystal X-ray techniques and microscopic examination of the reacting crystals. The crystal structure and solid-state conformation of aspirin anhydride were similar to those of related compounds. The crystal packing of aspirin anhydride allows the initial product of the solid-state reaction to be predicted; however, this prediction could not be tested because the thermal degradation products reported in the literature appear to be those obtained from reaction in a liquid state.
Keyphrases Aspirin anhydride-determination of crystal structure and solid-state behavior, X-ray crystallography and microscopy of reacting crystals 0 Crystal structure-aspirin anhydride, determination of solid-state behavior of crystals Degradation, thermal-aspirin anhydride end-products, crystal structure and solid-state behavior of aspirin anhydride determined
π SIMILAR VOLUMES
The main variables involved in solid-state polymerization of PET homopolymers, originally with molecular weight within the commercial range, were sequentially studied to determine their influence in polymerized products. These variables were precursor crystallinity, catalyst, and time and reaction t
The microkinetics of crystallization and the melting behavior of solid-state polymerized poly(ethylene terephthalate) (PET) have been studied. After correlating crystallization data with secondary nucleation theory and a single regime of growth, a positive correlation was found between molecular wei