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Crystal Structure and Solid State 13 C Nmr Analysis of Methyl 3,4,6-Tri- O -Acetyl-2-Deoxy-2-(3-Phenylureido)-β-D-Glucopyranoside

✍ Scribed by Anulewicz, Romana; Wawer, Iwona; Piekarska-Bartoszewicz, Boguslawa; Temeriusz, Andrzej

Book ID: 126646858
Publisher: Taylor and Francis Group
Year: 1999
Tongue: English
Weight: 478 KB
Volume: 18
Category: Article
ISSN: 0732-8303
DOI: 10.1080/07328309908544024

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Crystal structure and solid-state NMR an

Crystal structure and solid-state NMR analysis of methyl 2,3,6-tri-O-acetyl-2-deoxy-2-[3-(2-phenylethyl)-ureido]-β-d-glucopyranoside

✍ Roma Anulewicz; Iwona Wawer; Bogusława Piekarska-Bartoszewicz; Andrzej Temeriusz 📂 Article 📅 1996 🏛 Elsevier Science 🌐 English ⚖ 437 KB

The X-ray diffraction analysis of methyl 2,3,6-tri-O-acetyl-2-deoxy-2-[3-(2-phenylethyl)-ureido]-beta-D- glucopyranoside has been performed, establishing that molecules are associated by two types of NH...O hydrogen bonds, N-1-H with carbonyl-oxygen and N-3-H with anomeric oxygen, with N...O distanc

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NMR study of methyl 3,4,6-tri-O-acetyl-2-deoxy-2-(alkylureido)-β-D-glucopyranosides

✍ Iwona Wawer; Małgorzata Weychert; Jan Klimkiewicz; Bogusława Piekarska-Bartoszew 📂 Article 📅 1999 🏛 John Wiley and Sons 🌐 English ⚖ 117 KB 👁 1 views

Five derivatives of methyl 3,4,6-triacetyl-2-deoxy-(3@-dialkylureido)-b-D-glucopyranoside were studied by 1H and 13C, NMR spectroscopy in solutions and by 13C NMR spectroscopy in the solid state. Sterically CDCl 3 crowded substituents such as n-hexyl and cylcohexyl change the chemical shifts of H-1,

ChemInform Abstract: Crystal Structure a

ChemInform Abstract: Crystal Structure and Solid State NMR Analysis of N-(Methyl 3,4,6-tri- O-acetyl-2-amino-2-deoxy-β-D-glucopyranoside)-N′-carbamoyl-D- valine Ethyl Ester.

✍ R. ANULEWICZ; I. WAWER; B. PIEKARSKA-BARTOSZEWICZ; A. TEMERIUSZ 📂 Article 📅 2010 🏛 John Wiley and Sons ⚖ 30 KB 👁 2 views

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Single-crystal and powder X-ray diffract

Single-crystal and powder X-ray diffraction, 13C CP/MAS NMR, and DFT-GIAO calculations of methyl 3,4,6-tri-O-acetyl-2-O-(2,3,4,6-tetra-O-acetyl-β-d-galactopyranosyl)-α-d-glucopyranoside and methyl 2,4,6-tri-O-acetyl-3-O-(2,3,4,6-tetra-O-acetyl-β-d-galactopyranosyl)-α-d-glucopyranoside

✍ Gubica, Tomasz; Stępień, Dorota K.; Pisklak, Dariusz M.; Ostrowski, Andrzej; Cyr 📂 Article 📅 2013 🏛 Elsevier Science 🌐 English ⚖ 760 KB

Solid-state structure of methyl 2,4,6-tr

Solid-state structure of methyl 2,4,6-tri-O-acetyl-3-O-(2,3,4,6-tetra-O-acetyl-β-d-glucopyranosyl)-β-d-galactopyranoside and methyl 3,4,6-tri-O-acetyl-2-O-(2,3,4,6-tetra-O-acetyl-β-d-glucopyranosyl)-β-d-galactopyranoside

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13C, 15N CP MAS and high resolution mult

13C, 15N CP MAS and high resolution multinuclear NMR study of methyl 3,4,6-tri-O-acetyl-2-(3′-arylureido)-2-deoxy-β-d-glucopyranosides

✍ Iwona Wawer; Bogusława Piekarska-Bartoszewicz; Andrzej Temeriusz 📂 Article 📅 1996 🏛 Elsevier Science 🌐 English ⚖ 446 KB

Four new derivatives of methyl 3,4,6-triacetyl-2-deoxy-(3'-arylureido)-fl-D-glucopyranoside were studied by ~H, ~3C, ~SN NMR in CDC13 solutions and by ~3C, ~3N NMR in the solid state. The replacement of one aryl substituent by another has no influence on the proton and carbon chemical shifts within