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Crystal structure and paramagnetic properties of hexakis(pyridine N-oxide)nickel dibromate

✍ Scribed by Paduan-Filho, Armando.; Sinn, E.; Chirico, Robert D.; Carlin, Richard L.

Book ID: 127170187
Publisher: American Chemical Society
Year: 1981
Tongue: English
Weight: 466 KB
Volume: 20
Category: Article
ISSN: 0020-1669
DOI: 10.1021/ic50222a059

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## Abstract Pyridine‐2‐(3′‐mercaptopropanoic acid)‐__N__ ‐oxide (I), is a higher homologue of 1‐oxopyridinium‐2‐thioacetic acid (II) [1]. It crystallizes in monoclinic space group P2~1~ with a = 9.2168(2) Å, b = 4.1423(2) Å, c = 11.3904(4) Å, β = 98.65(2)°, V = 429.93(3) Å^3^ and Z = 2. The least‐s