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Crystal Structure and Characterization of [Ni(RPOEt)2(C2H5OH)2](ClO4)2[RPOEt

✍ Scribed by Pavica Planinić; Marijana Jurić; Berislav Perić; Marija Herceg

Book ID
106404544
Publisher
Springer
Year
2010
Tongue
English
Weight
432 KB
Volume
40
Category
Article
ISSN
1572-8854

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Crystal growth and characterization of Haldane chain compound Ni(C3H10N2)2NO2ClO4
✍ W. Tao; L.M. Chen; X.M. Wang; C. Fan; W.P. Ke; X.G. Liu; Z.Y. Zhao; Q.J. Li; X.F 📂 Article 📅 2011 🏛 Elsevier Science 🌐 English ⚖ 851 KB

The bulk single crystals of S ¼ 1 chain compound Ni(C 3 H 10 N 2 ) 2 NO 2 ClO 4 are grown by using a slow evaporation method at a constant temperature and a slow cooling method. It is found that the optimum condition of growing large crystals is via slow evaporation at 25 1C using 0.015 mol NiðClO 4