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Crystal-structure analysis using low-resolution nuclear magnetic resonance

✍ Scribed by I. K. Shmyrev; É. I. Fedin

Book ID
104921162
Publisher
SP MAIK Nauka/Interperiodica
Year
1971
Tongue
English
Weight
253 KB
Volume
11
Category
Article
ISSN
0022-4766

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The axial form of I5 N enriched aminocyclohexane has been detected at 173K, permitting the first direct measurement of the conformational free energy of the NH2 group. Relative intensities of individual conformer resonances in NMR spectra at low temperature, where ring inversion is estimates of the