Crystal and Molecule Structure of Piperidino-acet-m-Bromo-Anilide

✍ Scribed by Dr. L. Kutschabsky; Prof. Dr. H. Kriegsmann; P. Leibnitz; J. Wenzel

• Publisher: John Wiley and Sons
• Year: 1974
• Tongue: English
• Weight: 420 KB
• Volume: 9
• Category: Article
• ISSN: 0232-1300
• DOI: 10.1002/crat.19740090604

✦ Synopsis

Abstract

The compound piperidino‐acet‐m‐bromo‐anilide crystallizes in the orthorhombic space group Pbca with 8 molecules in the unit cell of dimensions a = 23.656; b = 12.664; c = 9.372 Å. The crystal structure was determined. The positions of all hydrogen atoms were located. The intermolecular hydrogen bond N(1)‐H(N1)… 0 has an influence on the conformation of the molecule. The angle between the plane of the phenyl ring and the plane of the carbonamide group is 36.8°.