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Crystal and molecular structure of p-methane triol(C10H20O3)

✍ Scribed by Vinod Singh Sambyal; K. N. Goswami; Tej P. Singh; R. K. Thappa


Publisher
John Wiley and Sons
Year
1994
Tongue
English
Weight
237 KB
Volume
29
Category
Article
ISSN
0232-1300

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✦ Synopsis


The compound crystallizes in the monoclinic crystal system with the space group P2,, having cell parameters u = 8.533(2) A, b = 10.388(2) A, c = 6.195(2) A, B = 92.17(1)". The structure has been solved by direct methods and refined upto R = 0.076. The six membered cyclo hexane ring is in chair conformation with maximum deviation 0.2296 8, for the C(1) atom. The molecules are held together by hydrogen bonding.


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Ethylenediamine trimolybdate, (C 2 H 10 N 2 ) [Mo 3 O 10 ], has been hydrothermally synthesized (180Β°C, 24 h, autogeneous pressure). It crystallizes in the monoclinic system (space group P2 1 /n) with a ‫؍‬ 8.0865(2) A s , b ‫؍‬ 14.4902(2) A s , c ‫؍‬ 8.9306(2) A s , ‫؍‬ 98.170(1)Β°, and Z ‫؍‬ 4. Its