Crystal and molecular structure of 7,7-dimethyl-2,3-di(4-methoxyphenyl)-5-oxo-5,6,7,8-tetrahydroquinoline
✍ Scribed by V. G. Kharchenko; L. I. Markova; Yu. T. Struchkov; A. A. Espenbetov; T. D. Kazarinova; N. T. Komyagin
- Publisher
- Springer US
- Year
- 1987
- Tongue
- English
- Weight
- 386 KB
- Volume
- 23
- Category
- Article
- ISSN
- 0009-3122
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📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 170 K Mean '(C±C) = 0.004 A Ê Disorder in main residue R factor = 0.047 wR factor = 0.139 Data-to-parameter ratio = 14.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
A green and convenient approach to the synthesis of novel 4,7-diaryl-2-oxo(thio)-1,2,3,4,5,6,7,8-octahydroquinazoline-5-one derivatives from appropriate aromatic aldehydes and 5-aryl-1,3-cyclohexanedione with urea or thiourea in the presence of dilute HCl as catalyst in water is described. This meth