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Crystal and molecular structure of 4-(phosphonemethyl)-2-hydroxy-2-oxo-1,4,2-oxazaphosphorinane and 4-(hydroxyethyl)-2-hydroxy-2-oxo-1,4,2-oxazaphosphorinane

✍ Scribed by B. I. Makaranets; T. N. Polynova; M. A. Porai-Koshits; S. A. Il'ichev

Publisher
SP MAIK Nauka/Interperiodica
Year
1987
Tongue
English
Weight
597 KB
Volume
27
Category
Article
ISSN
0022-4766

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## Abstract The title compound (C~14~H~10~N~2~O~2~Cl~2~) crystallizes in the monoclinic space group P2~1~/a with a=10.042(1) Γ…, b=10.317(1) Γ…, c=13.877(2) Γ…, Ξ²=97.36(2)Β°, V=1425.8(3) Γ…^3^, Z=4, D~x~=1.44 g.cm^‐3^. The structure was solved by direct methods and refined by full‐matrix least‐squares m