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Crystal and molecular structure of 4-(3-indolyl)butyric acid-picric acid 2/2 π complex

✍ Scribed by Manuel Soriano-García; Rubén Alfredo Toscano; Mario Schatz-Levin

Publisher
Springer
Year
1987
Tongue
English
Weight
646 KB
Volume
17
Category
Article
ISSN
1572-8854

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## Abstract The crystal structure of 4‐amino‐3‐(2‐benzothiophen) butyric acid is reported and compared with that of 4. amino‐3‐(2‐thiényl) butyric acid. For both molecules, the __γ__‐aminobutyric acid (GAB) chains show almost identical conformations. C~12~H~13~NO~2~S, Mw = 235.0, P2'~1~/c, a = 17.8

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✍ Carl-Gunnar Swahn; Håkan Beving; Göran Sedvall 📂 Article 📅 1978 🏛 John Wiley and Sons 🌐 French ⚖ 203 KB

The synthesis of the title compound is described. It involves base catalyzed substitution of deuterium for hydrogen in 3-p- -chlorophenylglutaric acid which is subsequently transformed to baclofen. The overall yield is 80%. ## INTRODUCTION AND DISCUSSION In order to develop a mass fragmentographi