Cross-polarization for quadrupolar nucle
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John C. Edwards; Paul D. Ellis
📂
Article
📅
1990
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John Wiley and Sons
🌐
English
⚖ 811 KB
## Abstract High‐field, ^95^Mo, solid‐state nuclear magnetic resonance spectra of (NH~4~)~6~Mo~7~O~24~ · 4H~2~O and (Bu~4~N)~2~Mo~2~O~7~ were obtained using solid‐echo techniques together with ^1^H cross‐polarization and dipolar decoupling. The results show that reliable second‐order powder line sh