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Cross-correlation suppressed T1and NOE experiments for protein side-chain13CH2groups

✍ Scribed by Changwen Jin; Jeanine J. Prompers; Rafael Brüschweiler


Book ID
110441728
Publisher
Springer Netherlands
Year
2003
Tongue
English
Weight
192 KB
Volume
26
Category
Article
ISSN
0925-2738

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A 3D triple resonance experiment has been designed to provide intraresidual and sequential correlations between amide nitrogens and c~-carbons in uniformly 13C/15N-labeled proteins. In-phase 13C~ magnetization is transferred to the aliphatic side-chain protons via the side-chain carbons using a CC-T