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CP-MAS and FT-IR spectroscopic studies of new derivatives of gossypol in solid

โœ Scribed by Piotr Przybylski; Grzegorz Bejcar; Wojciech Schilf; Bogumil Brzezinski; Franz Bartl

Publisher
Elsevier Science
Year
2005
Tongue
English
Weight
228 KB
Volume
751
Category
Article
ISSN
0022-2860

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CP/MAS spectroscopy in the determination
CP/MAS spectroscopy in the determination of the tautomeric forms of gossypol, its Schiff bases and hydrazones in the solid state
โœ Piotr Przybylski; Wojciech Schilf; Bohdan Kamienski; Bogumil Brzezinski; Franz B ๐Ÿ“‚ Article ๐Ÿ“… 2008 ๐Ÿ› John Wiley and Sons ๐ŸŒ English โš– 328 KB

## Abstract New Schiff bases and new hydrazones were synthesized and studied by ^13^C and ^15^N CP/MAS spectroscopy and by ^1^H๏ฃฟ^1^H COSY, ^1^H๏ฃฟ^13^C HMBC, ^1^H๏ฃฟ^13^C HSQC, ^1^H๏ฃฟ^15^N HMQC and ^1^H๏ฃฟ^15^N HSQC correlations. The CP/MAS investigation of gossypol has demonstrated that in the solid stat