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Coupled LC-GC: A new method for the on-line analysis of organochlorine pesticide residues in fat

✍ Scribed by Barcarolo, Roberto


Publisher
John Wiley and Sons
Year
1990
Tongue
English
Weight
407 KB
Volume
13
Category
Article
ISSN
0935-6304

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✦ Synopsis


Abstract

This paper describes the use of coupled LC‐GC for the determination of organochlorine pesticide residues in fat samples. Organochlorine pesticide residues are preseparated from fat by LC on a short C‐18 column using an organic solvent as the mobile phase. Evaporation of the LC eluent is achieved by a modified on‐column interface, introducing an on‐line vaporizer module using the fully concurrent evaporation technique.


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✍ José Luis Fernández Moreno; A. Garrido Frenich; Patricia Plaza Bolaños; José Lui 📂 Article 📅 2008 🏛 John Wiley and Sons 🌐 English ⚖ 224 KB 👁 1 views

## Abstract A new multiresidue method has been developed and validated for the determination of more than 140 pesticide residues in cucumber and orange by gas chromatography coupled to triple quadrupole mass spectrometry (GC–QqQ‐MS/MS) in a single run of 25.50 min. The triple quadrupole (QqQ) analy