Coupled HPLC-capillary GC - state of the art and outlook
✍ Scribed by Grob, K. ;Schilling, B.
- Publisher
- John Wiley and Sons
- Year
- 1985
- Tongue
- English
- Weight
- 810 KB
- Volume
- 8
- Category
- Article
- ISSN
- 0935-6304
No coin nor oath required. For personal study only.
✦ Synopsis
OH-Terminated Polysiloxane Stationary Phases somewhat more active surface for improved film stabilization. Accordingly, the columns with top separation efficiency are typically characterized by a slight activity caused by the support surface. For the first time, the new technique provides top separation efficiency combined with nearlyfull inertness as the result of an easy preparation procedure not requiring any extra effort.
Acknowledgment
For several years our work in column technology has been done in close collaboration with Prof. Kurt Grob. Without our work on his book, our long discussions and his help in rewriting this manuscript and rearranging the order of the material, this work could not have been published so soon.
I also wish to thank Art Mendicino and his colleagues from Ohio Valley Speciality Chemical Inc. for the preparation of all medium polar OH-terminated polysiloxanes introduced in this paper.
References
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