Correlation of thermal analysis and pyrolysis coupled to GC–MS in the characterization of tacrolimus
✍ Scribed by Tania Maria Böer; José Valdilânio Virgulino Procópio; Ticiano Gomes do Nascimento; Rui Oliveira Macêdo
- Book ID
- 118477626
- Publisher
- Elsevier Science
- Year
- 2013
- Tongue
- English
- Weight
- 715 KB
- Volume
- 73
- Category
- Article
- ISSN
- 0731-7085
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Taking advantage of the characteristic features of a thermal extraction unit for quantitative analysis, it has been possible to extend its utility to hrnace-type pyrolysis of polymers. Pyrolkis is achieved by accurate temperature programming of the pyrolysis cell from ambient to very high temperatur
## Abstract The thermal behavior of vitamin D~3~ was studied based on pyrolysis‐GC‐MS technique. It was pyrolyzed at 600 °C, 750 °C, 900 °C, respectively. The pyrolysis product were separated With an HP‐5 column and identified by the NIST mass spectral search program in combination with the correla