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Corrections-Linear Oligopeptides. Stereochemical Analysis of N-tert-Butyloxycarbonyl-L-prolylsarcosine and N-tert-Butyloxycarbonylsarcosylsarcosine in the Solid State and in Solution

✍ Scribed by Benedetti, Ettore; Ciajolo, Anna; DiBlasio, Benedetto; Pavone, Vincenzo; Pedone, Carlo; Toniolo, Claudio; Bonora, Gian

Book ID: 127386296
Publisher: American Chemical Society
Year: 1981
Tongue: English
Weight: 53 KB
Volume: 14
Category: Article
ISSN: 0024-9297
DOI: 10.1021/ma50002a601

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Linear Oligopeptides. 59. Stereochemical

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CONFORMATIONAL ANALYSIS OF N-(tert.-AMYL

CONFORMATIONAL ANALYSIS OF N-(tert.-AMYLOXYCARBONY-l-PROLINE IN THE SOLID STATE AND IN SOLUTION

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Conformational of Diastereoisomeric Pept

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Linear oligopeptides: 65′. Conformationa

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Preferred conformations of tert.-butylox

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## Abstract The X‐ray crystal structure of 1__H__‐pyrazole‐3‐(__N‐tert__‐butyl)‐carboxamide was determined. In the solid state, the ^13^C and ^15^N CP/MAS NMR spectra correspond to this tautomer. In solution, both tautomers are present in a ratio that depends on the temperature (at 293 K, 90% 3‐sub