Correction for anisotropic off-resonance decoupling effects in CPMAS of moderate susceptibility materials

✍ Scribed by T.K. Pratum

• Publisher: Elsevier Science
• Year: 1990
• Tongue: English
• Weight: 332 KB
• Volume: 172
• Category: Article
• ISSN: 0009-2614
• DOI: 10.1016/0009-2614(90)85405-2

✦ Synopsis

A simple decoupling method is presented which partially corrects for anisotropic off-resonance decoupling effects in magicangle-spinning NMR spectra (CPMAS) of magnetically inhomogeneous materials. This scheme is both simpler, and more effective than previously proposed broad band decoupling methods, and is applicable to 13C CPMAS of soils and related materials.