Copper(II) Complex of 1,10‐Phenanthroline Containing Two 5‐Fluorouracil Arranging in a New Way: Synthesis and Crystal Structure
✍ Scribed by Wu, Hui; Shen, Yang; Zhou, Jun; Yu, Kai‐bei
- Book ID
- 127341960
- Publisher
- Taylor and Francis Group
- Year
- 2006
- Tongue
- English
- Weight
- 214 KB
- Volume
- 36
- Category
- Article
- ISSN
- 0094-5714
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## Abstract A new complex, [Cu2(μ 2-Cl)2(IP)2Cl2] · 4H2O (IP = imidazo[4,5-f]1,10-phenathroline), was synthesised and characterised by elemental analysis, thermal analysis, IR spectra, and X-ray crystallography. The results showed that the complex crystallises in the monoclinic space group P $$ \ba
Blue crystals of Cu 2 (phen) 2 (H 2 O) 2 (C 5 H 6 O 4 ) 2 were obtained from a CH 3 OH±H 2 O solution containing CuCl 2 , 1,10-phenanthroline (phen), glutaric acid and Na 2 CO 3 . The crystal structure (monoclinic, P2 1 /c (no. 14), a = 10.271(1), b = 10.595(1), c = 15.585(1) A Ê , b = 107.105(3)°,