Copolyperoxides of 2-(acetoacetoxy)ethyl methacrylate with methyl methacrylate and styrene; Synthesis, characterization, thermal analysis, and reactivity ratios
β Scribed by Sunirmal Pal; Balaraju Banoth; Goli Rahithya; Ashish Dhawan; Priyadarsi De
- Book ID
- 116843537
- Publisher
- Elsevier Science
- Year
- 2012
- Tongue
- English
- Weight
- 701 KB
- Volume
- 53
- Category
- Article
- ISSN
- 0032-3861
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## Abstract A phthalimido group containing methacrylate based monomer 2β(__N__βphthalimido)ethyl methacrylate (NPEMA) was synthesized by reacting 2β(__N__βphthalimido)ethanol (NPE) with methacryloyl chloride. NPE was prepared by reacting phthalic anhydride dissolved in dimethyl formamide (DMF) with
Free-radical copolymerization of 4-nitrophenyl methacrylate (NPMA) with styrene (STY) was carried out at 65Β°C in 2-butanone by using benzoyl peroxide (BPO) as initiator. NPMA was characterized by spectral and microelemental analysis. Homoand copolymers were characterized by IR, 1 H-, and 13 C-NMR st