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Copolymerization of vinyl acetate with benzylidenemalononitrile

โœ Scribed by Kharas, Gregory ;Kohn, David H.

Publisher
John Wiley and Sons
Year
1984
Weight
270 KB
Volume
22
Category
Article
ISSN
0360-6376

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โœฆ Synopsis

Abstract

Vinyl acetate was copolymerized with benzylidenemalononitrile in bulk by radical initiation at 80ยฐC up to low conversions. Alternating copolymers were formed over a wide range of monomer feed ratios. The copolymerization parameters were determined by the conventional scheme. The copolymers were characterized by IR, proton, and ^13^C spectroscopy and their basic properties, solubility, viscosity, and thermal behavior were determined.

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With ammonium persulphate as initiator and Aerosol MA and Aerosol OT as emulsifiers, batch copolymerization of butyl acrylate and vinyl acetate (VAc) was investigated at 60 ยฐ, varying only the initial monomer feed composition. Accurate kinetic (polymerization rates, sequence distribution) and colloi