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Coordination Chemistry of the Nanocluster [HxPMo12O40⊂H4Mo72Fe30(O2CMe)15O254(H2O)98]

✍ Scribed by Douglas Ogrin; Andrew R. Barron

Book ID: 106406307
Publisher: Springer
Year: 2006
Tongue: English
Weight: 287 KB
Volume: 18
Category: Article
ISSN: 1040-7278
DOI: 10.1007/s10876-006-0088-3

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I : A suspension of 1 g of TiCI, in 15 mL of dry CH,CN was heated under reflux in an inert atmosphere (Ar) until a deep-blue solution was obtained. This was then treated dropwise with a solution of 1.2 g of N,N',N"-trimethyl-l,4,7-triazacyclononane (L) in 10 mL of CH,CN. After 30 minutes' stirring a