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Conversion of one hydroxy group in a diol to a phenyl ether with triphenylbismuth diacetate, a new glycol reaction showing strong axial preference in six-membered rings

✍ Scribed by David, Serge; Thieffry, Annie

Book ID: 126446945
Publisher: American Chemical Society
Year: 1983
Tongue: English
Weight: 1018 KB
Volume: 48
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo00152a007

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📜 SIMILAR VOLUMES

Selective phenylation in mild conditions

Selective phenylation in mild conditions of one hydroxy group in glycols with triphenylbismuth diacetate: A new specific glycol reaction.

✍ Serge David; Annie Thieffry 📂 Article 📅 1981 🏛 Elsevier Science 🌐 French ⚖ 221 KB

Refluxing for 4-5 h a dichloromethane solution of a diol in the presence of an equimolecular quantity of triphenylbismuth diacetate gave the monophenyl ether in good to excellent yield.