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Convenient synthesis of [η3-1- (formyl)allyl]- and [η3-1- (dimethoxymethyl)allyl]palladium chlorides

✍ Scribed by Sensuke Ogoshi; Kazuyoshi Hirako; Junji Nakanishi; Kouichi Ohe; Shinji Murai

Publisher
Elsevier Science
Year
1993
Tongue
English
Weight
233 KB
Volume
445
Category
Article
ISSN
0022-328X

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R-XC1, + 3 C(SilLle,), 7 R-X 3 LlCl v c1' -CI,C(SiMe,)> C(SiMe3)2 l a -c 2 3 a -c 4 c (20.6 g, 0.09 mol) cooled to -110°C. The mixture was stirred for 3 h, then treated with a solution of l c (6.57 g, 0.03 mol) in T H F (10 mL), and allowed to warm to -15°C. The solvents were then removed and the m