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Convenient Synthesis of Vinylsilanes and Their Use in Ketone Synthesis

✍ Scribed by Dipl.-Chem. Bengt-Thomas Gröbel; Prof. Dr. Dieter Seebach

Publisher
John Wiley and Sons
Year
1974
Tongue
English
Weight
215 KB
Volume
13
Category
Article
ISSN
0044-8249

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✦ Synopsis

Table 1. Condensation reactions between p-toluenesulfonates (R-OTos) and Grignard compounds (R'-Mu).

19 98 90 96 0 51 0 3 99 98 [a] OTs= OS01-ChH4-CH3. [b] Grignard reagent always added in excess (1.4 equiv.). [c] Glc analyses. internal reference substance: calibration factors for peak area correction: standard deviation f 3 %. [d] I 1 ), X = OTos. M g B r

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