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Convenient Synthesis of Thioctic Acid

✍ Scribed by Bullock, Milon W.; Hand, John J.; Stokstad, E. L. R.


Book ID
126192472
Publisher
American Chemical Society
Year
1957
Tongue
English
Weight
734 KB
Volume
79
Category
Article
ISSN
0002-7863

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## Abstract The reaction of phosgene or triphosgene with trimethylsilyl dialkylphosphites led to bisdialkylphosphonomethyl‐dialkylphosphates in good yields. The cleavage of the allyl ester was carried out under mild conditions using the Wilkinson catalyst. © 2003 Wiley Periodicals, Inc. Heteroatom