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Convenient route to niobium in lower oxidation states: synthesis and crystal structure of K4[Nb(C2O4)4] · 4H2O · 1/2H2C2O4

✍ Scribed by Bee-Lean Ooi; Takashi Shihabara; Genta Sakane; Kum-Fun Mok

Book ID
108328551
Publisher
Elsevier Science
Year
1997
Tongue
English
Weight
726 KB
Volume
266
Category
Article
ISSN
0020-1693

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Bis(disulfido) bridged Nb IV cluster oxalate complexes [Nb 2 (S 2 ) 2 (C 2 O 4 ) 4 ] 4± were prepared by ligand substitution reaction from the aqua ion [Nb 2 (l-S 2 ) 2 (H 2 O) 8 ] 4+ and isolated as K 4 (3). The crystal structures of 1 and 2 were determined. The crystals of 1 belong to the space