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Conformational study of catechol amine receptor sites. 7. Syntheses of erythro-and threo-3-amino-2-(3,4-dihydroxyphenyl)-2-butanol hydrochlorides and erythro- and threo-2-amino-3-(3,4-dihydroxyphenyl)butanehydrochlorides

โœ Scribed by Smissman, Edward E.; Borchardt, Ronald T.


Book ID
126935000
Publisher
American Chemical Society
Year
1971
Tongue
English
Weight
824 KB
Volume
14
Category
Article
ISSN
0022-2623

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X-ray and conformational investigations
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The crystafs of a 4:l mixture of 6-(N-benzyl-N-iert-butoxycarbonyIamino)-2,3,6,7-tetradeoxy~ a-aberythroand -p-oL-threa-hept-2-enopyranos-4-ulose were monoclinic, space group I??,/c, with cell dimensions: a = 9.490(2), h = 21.516(S), c = 10.279(2) A, p = 115.31(l)", Z = 4. The ulose ring had a half-