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Conformational and vibrational analysis of S-(2-methoxyphenyl)-4-substituted-benzenecarbothioates, using X-ray, infrared and Raman spectroscopy and theoretical calculations

✍ Scribed by I.C. Henao Castañeda; J.L. Jios; O.E. Piro; G.E. Tobón; C.O. Della Védova

Publisher: Elsevier Science
Year: 2007
Tongue: English
Weight: 541 KB
Volume: 842
Category: Article
ISSN: 0022-2860
DOI: 10.1016/j.molstruc.2006.12.007

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## Abstract Optically active threo‐(2S,4S)‐4‐mercapto‐2‐pentanol, erythro‐(2R,4S)‐4‐mercapto‐2‐pentanol and threo‐(2S,4S)‐pentanedithiol, were prepared from threo‐(2R,4R)‐pentanediol. The mechanism of their formation is discussed. The molecular optical rotation [M]~D~ of these compounds, of trans‐(