Conformational analysis of the series of 3(4)-halogen-substituted caran-4(3)-ols and 3-methylnorcaran-4(3)-OLS by their spectra
✍ Scribed by R. R. Shagidullin; É. Kh. Kazakova; S. V. Andreeva
- Book ID
- 112446071
- Publisher
- Springer
- Year
- 1987
- Tongue
- English
- Weight
- 255 KB
- Volume
- 36
- Category
- Article
- ISSN
- 1573-9171
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mixture was poured into ice-water(l00 ml) and extracted with CHC13(100 ml x 3). The extract was washed with H20, dried over MgS04 and evaporated to give Z-methylpropyl phenyl ketone(5d) as an oil(l6.20 g, 94%). 'H-NMR: 8.00(2H,dd,J=8.5 and 1.5Hz1, 7.60-7.23 (3H,m), 2.84(2H,d, J=6.8Hz), 2.40-2.08(lH,