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Conformational analysis of some substituted silatranyl-carboxylic acids produced by computational study and NMR spectroscopy

✍ Scribed by Xiaodong Zhang; Shizen Mao; Lianfang Shen; Chaohui Ye; Renxi Zhuo; Zhengrong Lu; G.A. Webb

Book ID
114141855
Publisher
Elsevier Science
Year
1995
Tongue
English
Weight
395 KB
Volume
372
Category
Article
ISSN
0166-1280

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✍ Rita Annunziata; Valentina Molteni; Laura Raimondi πŸ“‚ Article πŸ“… 1996 πŸ› John Wiley and Sons 🌐 English βš– 575 KB

The configuration and conformation of silyl ketene thioacetals derived from 2-pyridyl thioesters were studied by combined NMR and computational analysis. The results revealed that the (E)-silyl ketene thioacetal is always the thermodynamically favoured diastereoisomer; the equilibrium ratio is rever