✦ LIBER ✦

Configuration and conformation of a novel uridine analogue: 1H and 13C NMR spectra of (5'S)-1-[2'-(2-hydroxyethyl)tetrahydropyran-5'-yl]-1H-pyrimidine-2,4-dione

✍ Scribed by George Balayiannis; Dionissios Papaioannou; Anastassios Troganis

Publisher: John Wiley and Sons
Year: 2002
Tongue: English
Weight: 87 KB
Volume: 40
Category: Article
ISSN: 0749-1581
DOI: 10.1002/mrc.1001

No coin nor oath required. For personal study only.

✦ Synopsis

Abstract

A combination of homo‐ and heteronuclear 1D and 2D NMR techniques provided the assignment of the ^1^H and ^13^C resonances of the major component of a reaction product consisting of the two possible diastereomers of (5^′^S)‐1‐[2^′^‐(2‐hydroxyethyl)tetrahydropyran‐5^′^‐yl]‐1__H__‐pyrimidine‐2,4‐dione and showed that the tetrahydropyranyl ring in the major 5^′^S,2^′^S‐isomer adopts the twist conformation. Copyright © 2002 John Wiley & Sons, Ltd.

📜 SIMILAR VOLUMES

Syntheses of 4-[(1H,3H)-Pyrimidine-2,4-d

Syntheses of 4-[(1H,3H)-Pyrimidine-2,4-dion-1-yl]- and 4-[(1H,3H)-5-Methylpyrimidine-2,4-dion-1-yl]-1,6-heptadienes.

✍ Kamal H. Bouhadir; Jing-Lan Zhou; Philip B. Shevlin 📂 Article 📅 2005 🏛 John Wiley and Sons ⚖ 19 KB 👁 1 views

## Abstract For Abstract see ChemInform Abstract in Full Text.

1H and 13C NMR spectra of some 2-substit

1H and 13C NMR spectra of some 2-substituted 4,5-dimethylfurans

✍ Miloslava Dandárová; Daniel Végh 📂 Article 📅 1992 🏛 John Wiley and Sons 🌐 English ⚖ 202 KB

## Abstract ^1^H and ^13^C NMR spectra of 22 2‐substituted 4,5‐dimethylfurans are reported. The __J__(C, H) values were used for signal assignments and for the identification of geometrical isomers of some derivatives.

13C NMR spectra of 2,3-dihydro-1H-pyrrol

13C NMR spectra of 2,3-dihydro-1H-pyrrolo[1,2-c]imidazol-1,3-dione and its thione analogues

✍ Ronald S. Budhram; Barrie C. Uff; R. Alan Jones; Richard O. Jones 📂 Article 📅 1980 🏛 John Wiley and Sons 🌐 English ⚖ 221 KB

## Abstract Analysis of the ^13^C NMR spectra of a series of 2,3‐dihydro‐1__H__‐pyrrolo[1,2‐c]imidazole derivatives has provided chemical shift data for (˜184 ppm), (˜173.5 ppm), (˜158 ppm) and (˜148 ppm) groups. A full analysis of the ^13^C chemical shifts of the C atoms of the pyrrole ring an

NMR spectra and conformational analysis

NMR spectra and conformational analysis of substituted 1,3,4,5-tetrahydro-2H-1,5-benzodiazepin-2-one derivatives

✍ Farnaz Malik; Mashooda Hassan; Doris Rosenbaum; Helmut Duddeck 📂 Article 📅 1989 🏛 John Wiley and Sons 🌐 English ⚖ 400 KB

An investigation of the molecular dynamics of substituted 1,3,4,5-tetrahydro-2H-l,Ibenzodiazepin-2-0ne derivatives revealed that these molecules adopt cycloheptadiene-like boat conformations. There is an equilibrium between the quasi-axial and the quasiequatorial conformer in which the quasi-axial c

1H and 13C NMR Study of 1-Hydrazino-2,3-

1H and 13C NMR Study of 1-Hydrazino-2,3-dihydro-1H-pyrazolo[1,2-a]pyridazine-5,8-diones and -1H-pyrazolo[1,2-b]phthalazine-5,10-diones and Their Ring-Chain Tautomerism

✍ Jari Sinkkonen; Vladimir Ovcharenko; Kirill N. Zelenin; Irina P. Bezhan; Boris A 📂 Article 📅 2002 🏛 John Wiley and Sons 🌐 English ⚖ 135 KB 👁 1 views

Tautomeric behaviour and isotopic multip

Tautomeric behaviour and isotopic multiplets in the 13C NMR spectra of partially deuterated 5-arylazo-pyrimidine (1H,3H,5H)-2,4,6-triones and 5-arylazo-2-thioxo-pyrimidine (1H,3H,5H)-4,6-diones—evidence for elucidation of tautomeric forms

✍ Nader Noroozi Pesyan 📂 Article 📅 2009 🏛 John Wiley and Sons 🌐 English ⚖ 260 KB