✦ LIBER ✦

Concise procedure for the synthesis of cardiolipins having different fatty acid combinations

✍ Scribed by Masato Abe; Shigeki Kitsuda; Shunji Ohyama; Shinya Koubori; Masatoshi Murai; Hideto Miyoshi

Publisher: Elsevier Science
Year: 2010
Tongue: French
Weight: 257 KB
Volume: 51
Category: Article
ISSN: 0040-4039
DOI: 10.1016/j.tetlet.2010.02.071

No coin nor oath required. For personal study only.

✦ Synopsis

Production of a wide variety of cardiolipin (CL) analogues is critical for studying molecular mechanism of diverse biological functions of CL in mitochondria. We describe a concise procedure for the synthesis of CL using a phosphoramidite approach, which allows for the production of diverse CL analogues bearing linoleic acid(s) at any position on the glycerol backbone.

📜 SIMILAR VOLUMES

An improved procedure for the synthesis

An improved procedure for the synthesis of labelled fatty acids utilizing diethyl malonate

✍ Takhar Kasumov; Henri Brunengraber 📂 Article 📅 2006 🏛 John Wiley and Sons 🌐 French ⚖ 86 KB 👁 1 views

An improved procedure for the preparation and purification of labeled fatty acids by malonic ester synthesis has been developed. This method uses the different hydrolysis rates of the monoalkylmalonic ester intermediate and its dialkylmalonic ester side product. A convenient GC-MS monitoring techniq

Synthesis of esters of tetradecanoic aci

Synthesis of esters of tetradecanoic acid deuterated at the penultimate carbon: Some general procedures for the synthesis of selectively deuterated fatty acids

✍ P.W. Westerman; N. Ghrayeb 📂 Article 📅 1982 🏛 Elsevier Science 🌐 English ⚖ 368 KB

Methyl tetradecanoate, deuterated in the penultimate position has been prepared by three synthetic routes. One method in which an oxoester is an intermediate, utilizes the selective reducing properties of sodium borodeuteride and sodium cyanoborodeuteride towards oxo, tosyloxy and ester groups to in

An expeditious procedure for the synthes

An expeditious procedure for the synthesis of isotopically labelled fatty acids: preparation of 2,2-d2-nonadecanoic acid

✍ Annalisa Guaragna; Mauro De Nisco; Silvana Pedatella; Vittoria Pinto; Giovanni P 📂 Article 📅 2006 🏛 John Wiley and Sons 🌐 French ⚖ 152 KB

We describe a new synthetic path for the preparation of isotopically labelled saturated odd-numbered fatty acids by a homologation procedure for the direct conversion of carboxylic acids into their 2,2-dideuterated homologues. This process can be used to obtain both odd-and even-numbered 2,2-dideute

A Simple Procedure for the Regioselectiv

A Simple Procedure for the Regioselective Synthesis of Fatty Acid Esters of Maltose, Leucrose, Maltotriose and n-Dodecyl Maltosides

✍ Manuel Ferrer; M Angeles Cruces; Francisco J Plou; Manuel Bernabé; Antonio Balle 📂 Article 📅 2000 🏛 Elsevier Science 🌐 French ⚖ 150 KB

AbstractÐThe enzymatic acylation of several di-and trisaccharides with acyl donors ranging from 8 to 18 carbon atoms was carried out by transesteri®cation with the corresponding vinyl esters. The reaction was performed in 2-methyl-2-butanol/dimethylsulfoxide mixtures using the lipase from Humicola l

Annalisa Guaragna, Marc De Nisco, Silvan

Annalisa Guaragna, Marc De Nisco, Silvana Pedatella, Vittoria Pinto and Giovanni Palumbo, an expeditious procedure for the synthesis of isotopically labelled fatty acids: preparation of 2,2-d2-nonadecanoic acid. J Label Compd Radiopharm 2006; 49: 675–682

📂 Article 📅 2006 🏛 John Wiley and Sons 🌐 French ⚖ 55 KB

An expeditious procedure for the synthesis of isotopically labelled fatty acids: preparation of 2,2-d 2 -nonadecanoic acid COOH 15 CD 2 COOR 15