Computer system and flow cell for automated potentiometric and constant-current stripping analysis
β Scribed by Lars Renman; Daniel Jagner; Rickard Berglund
- Book ID
- 104100374
- Publisher
- Elsevier Science
- Year
- 1986
- Tongue
- English
- Weight
- 891 KB
- Volume
- 188
- Category
- Article
- ISSN
- 0003-2670
No coin nor oath required. For personal study only.
β¦ Synopsis
A flow cell and a personal computer-based system for potentiometric and constantcurrent stripping analysis are described. The thin-layer cell is designed for teflon-embedded glassy carbon electrodes in a spring-regulated holder, allowing simple instalment and leak-free behaviour. The personal computer is interfaced to hardware components such as potentiostat, amplifier, peristaltic pump, six inlet valves for different solutions, autosampler and strip-chart recorder. User-accessible commands allow electrolysis, stripping current, pump flow rates, valves, stripping transient recording, derivation, filtration and integration to be controlled, and through a number of user-defmed programs, to be performed in unattended operation. This I described by an example. Through a software interface to a high-level language (BASIC), results from any number of analytical runs can be further evaluated by standard addition, or from calibration curves, or by statistical methods.
π SIMILAR VOLUMES
A flow system for voltammetric analysis is described and characterized. This system was designed so that sample manipulation and electrochemical experiments could be performed under automated control. The goal of this work is to expand the practical possibilities for elucidation of the electrochemic