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Comprehensive and Cost-Effective NMR Spectroscopy of Methyl Groups in Large Proteins

✍ Scribed by Otten, Renee; Chu, Byron; Krewulak, Karla D.; Vogel, Hans J.; Mulder, Frans A. A.

Book ID
118018572
Publisher
American Chemical Society
Year
2010
Tongue
English
Weight
410 KB
Volume
132
Category
Article
ISSN
0002-7863

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A quadruple-quantum filtered HSQC ( QQF-HSQC ) for the and demonstrated in practice on the 14-kDa human nonpancreatic synovial phospholipase A2 ( hnps-PLA2 ) . The constant-time selection of methyl groups which minimizes the line-broadening effects of proton homonuclear couplings is presented. The s