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Compounds with Cluster Cations together with Cluster Anions [(M6X12)(EtOH)6]2+ besides [(Mo6Cl8)Cl4X2]2– (M = Nb, Ta; X = Cl, Br) – Synthesis and Crystal Structures

✍ Scribed by I. Bašic; N. Brničević; U. Beck; A. Simon; R. E. McCarley


Publisher
John Wiley and Sons
Year
1998
Tongue
German
Weight
179 KB
Volume
624
Category
Article
ISSN
0372-7874

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✦ Synopsis


Compounds consisting of both cluster cations and cluster anions of the composition [(M 6 X 12 )(EtOH) 6 ][(Mo 6 Cl 8 )Cl 4 X 2 ] ´n EtOH ´m Et 2 O (M = Nb, Ta; X = Cl, Br) have been prepared by the reaction of (M 6 X 12 )X 2 ´6 EtOH with (Mo 6 Cl 8 )Cl 4 . IR data are given for three compounds. The structures of [(Nb 6 Cl 12 )(