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Composition of Iodopropylideneglycerol: an Example of the Application of 2D NMR Spectroscopy to Structure Elucidation

✍ Scribed by A. Virgili; J. Cervelló

Publisher
John Wiley and Sons
Year
1996
Tongue
English
Weight
346 KB
Volume
34
Category
Article
ISSN
0749-1581

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✦ Synopsis

Using 1D and 2D NMR spectra, the compounds obtained, in a mixture, in the reaction of glycerol with iodine were identified as the two isomers (cis and trans) of 2-iodomethyl-5-hydroxymethyl-1,4-dioxane and the two isomers (cis and trans) of 2-iodomethyl-6-hydroxymethyl-1,4-dioxane. Thus, the composition of the pharmaceutical formulation named IPG has finally been established.

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